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BASi LCEC Flowcells

BASi has developed a variety of flow cells to fit a variety of applications. How do you make a choice? To begin, the analyte in most cases determines the working electrode material. For most oxidizable/reducible organic compounds, a glassy carbon electrode is used, for acetylcholine a platinum or “wired” glassy carbon is used(since enzymatic derivatization yields H2O2 for detection), Hg/Au is used to determine thiols/disulfides, a copper electrode for carbohydrates, gold for pulsed electrochemical techniques-call BASi and we will discuss detection of your analyte.

Second, is the column of standard size or is it microbore? In many instances a cell used for standard chromatography can be optimized for a microbore system by the simple change of gasket thickness-thus reducing the cell-dead-volume. What flow pattern, cross-flow or radial-flow, will give optimal response, thus resulting in lower detection limits? Generally radial-flow cells are best suited for microbore systems and cross-flow for standard systems. If fraction collection or connection to a second detector (UV, fluorescence, or MS) is required, then the cross-flow with reference port configuration (MF-1092) should be used.

The following sections describe a number of options. Call BASi if it is not clear to you which cell best fits your system/application. A complete flowcell consists of two separate BASi part numbers:

  • The Auxiliary Electrode includes a phenolic base, arms, and exit tube.

  • The Cell Kit includes a glassy carbon working electrode, gasket, reference electrodes, the retaining hardware for these electrodes, and a polishing kit.

In many cases several types of Cell Kits are compatible with a particular Auxiliary Electrode.

Flowcells

To purchase a complete Flowcell, order an Auxiliary Electrode and a Cell Kit.

Flow Pattern


Cross

Arc

Radial

 
Auxiliary Electrodes


MF-1093


MF-1092


MF-1087

MF-1091

 
Cell Kits


MW-5052


MW-5050


MW-5051

 

Replacement Gaskets and Working Electrodes

Flow Pattern


Cross

Arc

Radial

 
Cell Gaskets


0.0005" MF-1044
0.002" MF-1046
0.005" MF-1047
0.015" MF-1048

0.0005" MF-1067
0.002" MF-1066

0.0005" MF-1068
0.002" MF-1069

 
Working Electrode Blocks


MF-1095


MF-1000


MF-1085


MF-1086


MF-1095


MF-1085


MF-1015